University of the Basque Country University of the Basque Country

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GENERAL NUCLEAR MAGNETIC RESONANCE OF THE UPV/EHU

Equipment

The NMR Service equipment comprises eight instruments in total, three of which can be considered routine (300 MHz, samples in solution) and operate exclusively on a self-service basis for basic research at the UPV/EHU. The two 500 MHz pieces of equipment (located in San Sebastián and Leioa), two 400 MHz equipment (three channels/CPMAS) in Vitoria (19F-roadband San Sebastian), and one spectrometer for solid state sample 400Mhz equipment located in San Sebastián, are those set aside for the provision of external services.

  • Liquid state NMR (300-400 & 500 MHZ).
  • Solid state NMR (400 MHZ)

Bruker AVANCE 5OO (two-bay)

  • Two-channel console with gradients (50G/cm) on Z axis.
  • Two-channel inverse detection probe BBI 1H / 31P- 109 Ag gradients on the Z axis. Temperature interval: -100 °C +180 °C.
  • Two-channel direct detection probe BBO 1H / 31P- 15 N gradients on the Z axis. Temperature interval: -100 °C +180 °C.
  • Two-channel direct detection probe BBO 1H-19F / 31P- 15 N gradients on the Z axis. Temperature interval: -100 °C +180 °C.
  • High-precision temperature control unit -150 to +400 °C. Gas conditioning system with a work interval from -10 °C to +9 0°C. Additional gas conditioning system with a work interval from +20 °C to -150 °C.
  • PC control computer with Linux
  • Location: Joxe Mari Korta R&D Centre

Bruker AVANCE 5OO (one-bay)

  • Two-channel console with gradients (50G/cm) on Z axis.
  • Two-channel inverse detection probe BBI 1H / 31P- 109Ag gradients on the Z axis. Temperature interval: -100 °C +180 °C.
  • High-precision temperature control from -150 to +400 °C. Gas conditioning system with a work interval from -10 °C to +90 °C. Additional gas conditioning system with a work interval from +20 °C to -150 °C.
  • PC control computer with Windows
  • Location: Faculty of Science and Technology Leioa

Bruker AVANCE 4OO

  • Three-channel console with gradients (50G/cm) on Z axis.
  • 5mm QNP probe pre-tuned for (1H/13C/19F/31P) with gradients on the Z axis. Temperature interval: -150 °C  +180 °C.
  • High-precision temperature control unit from -150 to +400 °C. Gas conditioning system with a work interval from -10 °C to +90 °C. Additional gas conditioning system with a work interval from +20 °C to -150 °C.
  • PC control computer
  • Location: Pharmacy Faculty Vitoria-Gasteiz

Bruker AVANCE II 400

  • Two-channel console with gradient (50G/cm) in axis Z two channel, direct detection BBO ^1 H-^19 F / ^31 P- ^15 N (Z axis gradient). Temperature interval : -100°C +180 °C.
  • Unidad de control de temperatura de alta precisión -150 hasta +400 °C. Sistema de acondicionamiento de gases con una intervalo de trabajo de -10 °C hasta +90 °C. Sistema de acondicionamiento de gases adicional con un intervalo de trabajo de +20 °C a -150 °C
  • PC control computer with Linux
  • Location: Joxe Mari Korta R&D Centre

Bruker AVANCE 300

  • Two-channel console.
  • Broadband two-channel probe BBO 31P- 109Ag/1H . Temperature interval: -100 °C  +180 °C. Suitable for studying heteronuclei.
  • High-precision temperature control unit from -150 to +400°C. Gas conditioning system with a work interval from -10°C to +90°C. Additional gas conditioning system with a work interval from +20°C to -150°C
  • PC computer control with Linux
  • Location: Chemistry Faculty Donostia

Varian Unity 3OO

Bruker Avance II 300

  • Two-channel console with gradients (50G/cm) on Z axis.
  • 5mm QNP probe pre-tuned for (1H/13C/19F/31P) with gradients on the Z axis. Temperature interval: -150 °C +150 °C.
  • Temperature control unit with a work interval from –150 °C to +300 °C.
  • PC computer control with Linux.
  • Location: Faculty of Science and Technology Leioa

Bruker AVANCE III 400

  • Three channel console.
  • 1.3 mm probe high speed (60 KHz) ^1 H-^19 F / X. Temperature interval: -30 °C +70 °C.
  • 4 mm probe for solid sample (CP-MAS) ^1 H-^19 F / X / Y ( ^13 C, ^15 N,^31 P, ^27 Al,^29 Si ) Temperature interval : -150 °C +180 °C.
  • 7 mm probe for solid samples (CP-MAS) ^1 H / X( ^31 P- ^15 N). Temperature interval : -150 °C 180 °C.
  • High-precision temperature control unit from -270 °C to +400 °C. Gas conditioning system with a work interval from -10 °C to +90 °C. Gas conditioning system with a work interval from -150 °C to 20 °C.
  • PC control computer with Linux
  • Location: Joxe Mari Korta R&D Centre